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When the 1V-LSD hemitartrate salt was subjected to basification and extraction with diethyl ether prior to GC-MS analysis, it was discovered that hydrolysis to LSD happened (Supporting Information and facts). On top of that, three more 1V-LSD isomers had been detected within the GC-MS TIC trace with 1V-LSD labeled as isomer I. In the event the 1V-L